From ebbc9a27a0b132e5bd3a3caf81c636ecd99eddc8 Mon Sep 17 00:00:00 2001 From: RemDelaporteMathurin Date: Mon, 23 Dec 2024 14:50:50 -0500 Subject: [PATCH 1/2] add repeat samples for 1-1 and 1-2 --- data/tritium_detection/REPEAT_IV-1-1_1-2.csv | 86 ++++++++++++++++++++ 1 file changed, 86 insertions(+) create mode 100644 data/tritium_detection/REPEAT_IV-1-1_1-2.csv diff --git a/data/tritium_detection/REPEAT_IV-1-1_1-2.csv b/data/tritium_detection/REPEAT_IV-1-1_1-2.csv new file mode 100644 index 0000000..1b18690 --- /dev/null +++ b/data/tritium_detection/REPEAT_IV-1-1_1-2.csv @@ -0,0 +1,86 @@ +Assay Definition + +Assay Description: +Low-level assay for 3H in UG LLT +Assay Type: DPM (Single) +Report Name: Report1 +Output Data Path: C:\Packard\TriCarb\Results\Default\Flibe_Test\Various +Raw Results Path: C:\Packard\Tricarb\Results\Default\Flibe_Test\20241221_0801\20241221_0801.results +Comma-Delimited File Name: C:\Packard\TriCarb\Results\Default\Flibe_Test\Various\REPEAT_IV-1-1_1-2.csv +Assay File Name: C:\Packard\TriCarb\Assays\Flibe_Test.lsa + + +Count Conditions + +Nuclide: 3H UG LLT Normal + Quench Indicator: tSIE/AEC + External Std Terminator (sec): 0.5 2s% + Pre-Count Delay (min): 0.00 +Quench Set: + Low Energy: 3H-UG-LLT-NM +Count Time (min): 100.00 +Count Mode: Normal +Assay Count Cycles: 1 Repeat Sample Count: 6 +Number of Vials/Sample: 1 Calculate % Reference: Off + + +Background Subtract: Off +Low CPM Threshold: Off +2 Sigma % Terminator: Off + +Regions LL UL +A 0.0 18.6 +B 2.0 18.6 +C 4.0 18.6 + + +Count Corrections + +Static Controller: On Luminescence Correction: On GCT: n/a +Colored Samples: Off Heterogeneity Monitor: Off PAC: Disabled +Coincidence Time (nsec): 18 Delay Before Burst (nsec): 75 PAC Strength: n/a Auxiliary Spectrum: n/a + + +S#,SMPL_ID,Bq:1,CPMA,LUM,tSIE,Eff Nuc1 In A,Count Time,DPM1 +1,1L-Bl-1,0.366,6,0,286.57,26.46,100.00,22 +1,1L-Bl-1,0.365,6,0,283.77,26.22,100.00,22 +1,1L-Bl-1,0.337,5,0,285.04,26.33,100.00,20 +1,1L-Bl-1,0.349,5,0,283.57,26.21,100.00,21 +1,1L-Bl-1,0.366,6,0,285.64,26.38,100.00,22 +1,1L-Bl-1,0.351,6,0,285.39,26.36,100.00,21 +,,0.356,6,0,285.00,26.33,,21 + +Missing vial 2. +3,1L-IV_1-1-3,1.714,27,0,283.52,26.20,100.00,103 +3,1L-IV_1-1-3,1.689,27,0,283.75,26.22,100.00,101 +3,1L-IV_1-1-3,1.681,26,0,284.01,26.24,100.00,101 +3,1L-IV_1-1-3,1.728,27,0,283.58,26.21,100.00,104 +3,1L-IV_1-1-3,1.754,28,0,283.25,26.18,100.00,105 +3,1L-IV_1-1-3,1.702,27,0,283.99,26.24,100.00,102 +,,1.711,27,0,283.68,26.22,,103 + +4,1L-IV_1-1-4,0.415,7,0,284.33,26.27,100.00,25 +4,1L-IV_1-1-4,0.413,6,0,283.74,26.22,100.00,25 +4,1L-IV_1-1-4,0.428,7,0,283.92,26.24,100.00,26 +4,1L-IV_1-1-4,0.416,7,0,283.91,26.24,100.00,25 +4,1L-IV_1-1-4,0.403,6,0,283.70,26.22,100.00,24 +4,1L-IV_1-1-4,0.417,7,0,284.34,26.27,100.00,25 +,,0.415,7,0,283.99,26.24,,25 + +Missing vial 5. +6,1L-IV_1-2-3,3.487,54,0,280.88,25.98,100.00,209 +6,1L-IV_1-2-3,3.427,53,0,281.31,26.01,100.00,206 +6,1L-IV_1-2-3,3.371,53,0,281.33,26.01,100.00,202 +6,1L-IV_1-2-3,3.490,55,0,281.77,26.05,100.00,209 +6,1L-IV_1-2-3,3.482,54,0,282.11,26.08,100.00,209 +6,1L-IV_1-2-3,3.309,52,0,282.00,26.07,100.00,199 +,,3.428,54,0,281.57,26.04,,206 + +7,1L-IV_1-2-4,0.645,10,0,282.01,26.07,100.00,39 +7,1L-IV_1-2-4,0.628,10,0,283.07,26.16,100.00,38 +7,1L-IV_1-2-4,0.620,10,0,282.85,26.14,100.00,37 +7,1L-IV_1-2-4,0.615,10,0,283.22,26.18,100.00,37 +7,1L-IV_1-2-4,0.650,10,0,283.43,26.19,100.00,39 +7,1L-IV_1-2-4,0.627,10,0,284.45,26.28,100.00,38 +,,0.631,10,0,283.17,26.17,,38 + From 95fc9e77a6afacb1a74f6c762cf0310318243088 Mon Sep 17 00:00:00 2001 From: RemDelaporteMathurin Date: Fri, 3 Jan 2025 09:40:37 -0500 Subject: [PATCH 2/2] added repeat test in low-level count mode --- .../REPEAT_LOW_IV-1-1_1-2.csv | 86 +++++++++++++++++++ 1 file changed, 86 insertions(+) create mode 100644 data/tritium_detection/REPEAT_LOW_IV-1-1_1-2.csv diff --git a/data/tritium_detection/REPEAT_LOW_IV-1-1_1-2.csv b/data/tritium_detection/REPEAT_LOW_IV-1-1_1-2.csv new file mode 100644 index 0000000..168d475 --- /dev/null +++ b/data/tritium_detection/REPEAT_LOW_IV-1-1_1-2.csv @@ -0,0 +1,86 @@ +Assay Definition + +Assay Description: +Repeat count low-level assay for 3H in UG LLT +Assay Type: DPM (Single) +Report Name: Report1 +Output Data Path: C:\Packard\TriCarb\Results\Default\Flibe_Test\Various +Raw Results Path: C:\Packard\Tricarb\Results\Default\Flibe_Test\20241224_0109\20241224_0109.results +Comma-Delimited File Name: C:\Packard\TriCarb\Results\Default\Flibe_Test\Various\REPEAT_LOW_IV-1-1_1-2.csv +Assay File Name: C:\Packard\TriCarb\Assays\Flibe_Test.lsa + + +Count Conditions + +Nuclide: 3H UG LLT Low Level + Quench Indicator: tSIE/AEC + External Std Terminator (sec): 0.5 2s% + Pre-Count Delay (min): 0.00 +Quench Set: + Low Energy: 3H-UG-LLT +Count Time (min): 100.00 +Count Mode: Low Level +Assay Count Cycles: 1 Repeat Sample Count: 6 +Number of Vials/Sample: 1 Calculate % Reference: Off + + +Background Subtract: Off +Low CPM Threshold: Off +2 Sigma % Terminator: Off + +Regions LL UL +A 0.0 18.6 +B 2.0 18.6 +C 4.0 18.6 + + +Count Corrections + +Static Controller: On Luminescence Correction: On GCT: n/a +Colored Samples: Off Heterogeneity Monitor: Off PAC: Disabled +Coincidence Time (nsec): 18 Delay Before Burst (nsec): 75 PAC Strength: n/a Auxiliary Spectrum: n/a + + +S#,SMPL_ID,Bq:1,CPMA,LUM,tSIE,Eff Nuc1 In A,Count Time,DPM1 +1,1L-Bl-1,0.250,3,1,285.91,22.52,100.00,15 +1,1L-Bl-1,0.238,3,0,285.58,22.49,100.00,14 +1,1L-Bl-1,0.257,3,0,287.13,22.61,100.00,15 +1,1L-Bl-1,0.255,3,0,287.11,22.61,100.00,15 +1,1L-Bl-1,0.257,3,0,286.91,22.59,100.00,15 +1,1L-Bl-1,0.258,4,0,287.72,22.65,100.00,16 +,,0.253,3,0,286.73,22.58,,15 + +Missing vial 2. +3,1L-IV_1-1-3,1.630,22,0,285.28,22.47,100.00,98 +3,1L-IV_1-1-3,1.530,21,0,285.91,22.52,100.00,92 +3,1L-IV_1-1-3,1.578,21,0,285.17,22.46,100.00,95 +3,1L-IV_1-1-3,1.545,21,0,285.70,22.50,100.00,93 +3,1L-IV_1-1-3,1.500,20,0,284.90,22.44,100.00,90 +3,1L-IV_1-1-3,1.622,22,0,284.49,22.41,100.00,97 +,,1.567,21,0,285.24,22.47,,94 + +4,1L-IV_1-1-4,0.313,4,1,285.57,22.49,100.00,19 +4,1L-IV_1-1-4,0.323,4,1,285.51,22.49,100.00,19 +4,1L-IV_1-1-4,0.342,5,1,285.29,22.47,100.00,20 +4,1L-IV_1-1-4,0.326,4,1,286.53,22.56,100.00,20 +4,1L-IV_1-1-4,0.328,4,0,286.35,22.55,100.00,20 +4,1L-IV_1-1-4,0.334,5,1,287.28,22.62,100.00,20 +,,0.328,4,1,286.09,22.53,,20 + +Missing vial 5. +6,1L-IV_1-2-3,3.371,45,0,283.74,22.36,100.00,202 +6,1L-IV_1-2-3,3.283,44,0,285.49,22.49,100.00,197 +6,1L-IV_1-2-3,3.270,44,0,284.47,22.41,100.00,196 +6,1L-IV_1-2-3,3.226,43,0,284.87,22.44,100.00,194 +6,1L-IV_1-2-3,3.282,44,0,281.40,22.18,100.00,197 +6,1L-IV_1-2-3,3.387,45,0,281.59,22.20,100.00,203 +,,3.303,44,0,283.59,22.35,,198 + +7,1L-IV_1-2-4,0.571,8,1,284.81,22.44,100.00,34 +7,1L-IV_1-2-4,0.534,7,1,283.63,22.35,100.00,32 +7,1L-IV_1-2-4,0.558,7,1,284.10,22.38,100.00,33 +7,1L-IV_1-2-4,0.521,7,1,284.76,22.43,100.00,31 +7,1L-IV_1-2-4,0.537,7,1,283.03,22.30,100.00,32 +7,1L-IV_1-2-4,0.522,7,1,285.37,22.48,100.00,31 +,,0.541,7,1,284.28,22.40,,32 +